5V49
Trypanosoma brucei methionyl-tRNA synthetase in complex with inhibitor (Chem 1917)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-28 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 87.190, 106.200, 207.520 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 103.760 - 2.300 |
R-factor | 0.20642 |
Rwork | 0.205 |
R-free | 0.22849 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.347 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 103.760 |
High resolution limit [Å] | 2.300 |
Rmerge | 0.169 |
Number of reflections | 86365 |
<I/σ(I)> | 8.1 |
Completeness [%] | 100.0 |
Redundancy | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 2.0 M ammonium sulfate, 0.2 M sodium chloride, 0.1 M sodium cacodylate, pH 6.2, VAPOR DIFFUSION, SITTING DROP, temperature 298K |