5V3O
Cereblon in complex with DDB1 and CC-220
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-04-11 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9787 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 111.029, 126.886, 172.487 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.010 - 3.200 |
R-factor | 0.20693 |
Rwork | 0.204 |
R-free | 0.26733 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.506 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.010 |
High resolution limit [Å] | 3.200 |
Rmerge | 0.089 |
Number of reflections | 40911 |
<I/σ(I)> | 19.8 |
Completeness [%] | 100.0 |
Redundancy | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 200mM NaCl, 20% PEG 3350 |