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5UHA

Crystal structure of Mycobacterium tuberculosis transcription initiation complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyPIXEL
Collection date2016-04-09
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.925
Spacegroup nameP 21 21 21
Unit cell lengths150.197, 163.481, 195.653
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution48.913 - 3.906
R-factor0.2149
Rwork0.211
R-free0.27910
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0004.040
High resolution limit [Å]3.9008.3903.900
Rmerge0.2190.110
Rmeas0.2260.113
Rpim0.0570.0250.387
Total number of observations659212
Number of reflections44080
<I/σ(I)>3.6
Completeness [%]99.29999.4
Redundancy15208.2
CC(1/2)0.9940.144
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.229550 mM Tris-HCl, pH 8.2, 200 mM KCl, 50 mM MgCl2, and 10% PEG3350

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