5UFO

Structure of RORgt bound to

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	80
Detector technology	PIXEL
Collection date	2015-03-30
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1
Spacegroup name	P 61 2 2
Unit cell lengths	88.811, 88.811, 144.257
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	37.814 - 2.802
R-factor	0.196
Rwork	0.191
R-free	0.24350
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.582
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	37.814
High resolution limit [Å]	2.800
Number of reflections	8782
<I/σ(I)>	22.4
Completeness [%]	99.8
Redundancy	17.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	1.35M NaFormate, 0.1M Hepes pH7, 3%MPD