5UE5
proMMP-7 with heparin octasaccharide bound to the catalytic domain
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III | 800 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D 1H-15N NOESY |
| 2 | 1 | 1 | TROSY-detected titration |
| 3 | 2 | 2 | PREs by PROJECT-CPMG TROSY |
| 4 | 3 | 4 | solvent PREs, 1H relaxation detected via TROSY |
| 5 | 4 | 5 | 3D HNCACB |
| 6 | 4 | 5 | 3D CBCA(CO)NH |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.6 | 1 | 310 |
| 2 | 6.6 | 1 | 310 |
| 3 | 6.6 | 1 | 310 |
| 4 | 6.6 | 1 | 310 |
Conformers
| Conformers Calculated Total Number | 200 |
| Conformers Submitted Total Number | 16 |
