Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-BM-C |
| Synchrotron site | APS |
| Beamline | 14-BM-C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-02-13 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9 |
| Spacegroup name | P 21 3 |
| Unit cell lengths | 188.792, 188.792, 188.792 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 84.430 - 2.000 |
| R-factor | 0.1831 |
| Rwork | 0.176 |
| R-free | 0.20600 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.868 |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 2.070 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.132 | 0.532 |
| Number of reflections | 148902 | |
| Completeness [%] | 99.0 | 98.8 |
| Redundancy | 40 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 3.4~4.0 M sodium formate, 50 mM Tris, pH 7.5 |
