5T8F
p110delta/p85alpha with taselisib (GDC-0032)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-01-17 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.99988 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 91.096, 108.604, 142.223 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 86.370 - 2.910 |
R-factor | 0.243 |
Rwork | 0.242 |
R-free | 0.30400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5dxu |
RMSD bond length | 0.008 |
RMSD bond angle | 1.121 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.370 | 3.160 |
High resolution limit [Å] | 2.910 | 2.910 |
Rmerge | 0.044 | |
Number of reflections | 31603 | |
<I/σ(I)> | 20.4 | 5.6 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 8.1 | 8.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG |