5T7L
Pt(II)-mediated copper-dependent interactions between ATOX1 and MNK1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-28 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0597 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.617, 54.659, 63.719 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.486 - 2.830 |
R-factor | 0.2035 |
Rwork | 0.200 |
R-free | 0.27340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cjk |
RMSD bond length | 0.009 |
RMSD bond angle | 1.150 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | Sir2014 |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.490 | 2.931 |
High resolution limit [Å] | 2.830 | 2.830 |
Rmerge | 0.107 | |
Number of reflections | 4184 | |
<I/σ(I)> | 7.58 | 2.41 |
Completeness [%] | 98.1 | 92.77 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG-6000 10 to 30 % w/v and sodium citrate 0.1M at pH 4.7 | |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG-6000 10 to 30 % w/v and sodium citrate 0.1M at pH 4.7 |