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5Q0M

Ligand binding to FARNESOID-X-RECEPTOR

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyCCD
Collection date2008-09-04
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.0
Spacegroup nameP 65
Unit cell lengths93.562, 93.562, 45.590
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution40.514 - 2.200
R-factor0.1869
Rwork0.183
R-free0.26150
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle1.024
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Refinement softwarePHENIX
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]46.8002.300
High resolution limit [Å]2.2002.200
Rmerge0.0620.543
Number of reflections117521454
<I/σ(I)>12.611.86
Completeness [%]99.999.5
Redundancy4.143.59
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1evaporation, hanging drop7.52980.1 M HEPES pH 7.5, 1.4 M Sodium Citrate

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