5OWR
Human STK10 bound to dasatinib
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-10-05 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9795 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 49.740, 111.720, 133.150 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 85.580 - 2.300 |
R-factor | 0.22146 |
Rwork | 0.220 |
R-free | 0.25362 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | STK10 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.180 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 85.580 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.100 | 1.030 |
Number of reflections | 16890 | 7139 |
<I/σ(I)> | 37.2 | 1.7 |
Completeness [%] | 99.9 | 100 |
Redundancy | 4.3 | 4.3 |
CC(1/2) | 0.997 | 0.667 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 40% PEG 300, 0.20M Ca(ac)2, 0.1M cacodylate pH 6.5 |