5OU3
M. thermoresistible IMPDH in complex with IMP and Compound 31 (AT080)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 77 |
Detector technology | PIXEL |
Collection date | 2016-06-22 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.98 |
Spacegroup name | I 4 |
Unit cell lengths | 89.280, 89.280, 85.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.150 - 1.600 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 36.150 |
High resolution limit [Å] | 1.600 |
Number of reflections | 43461 |
<I/σ(I)> | 9.31 |
Completeness [%] | 100.0 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 292 | 100mM sodium acetate pH 5.5, 200mM calcium chloride, 8-14% iso-propanol |