5OCV

A Rare Lysozyme Crystal Form Solved Using High-Redundancy 3D Electron Diffraction Data from Micron-Sized Needle Shaped Crystals

Experimental procedure

Temperature [K]	97
Spacegroup name	P 21 21 2
Unit cell lengths	67.720, 103.880, 31.650
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.673 - 2.200
R-factor	0.2382
Rwork	0.236
R-free	0.27000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1aki
RMSD bond length	0.002
RMSD bond angle	0.550
Data reduction software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.11.1_2575: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	28.680	2.280
High resolution limit [Å]	2.200	2.200
Number of reflections	9516
Completeness [%]	79.7	64.3
Redundancy	42.4	25.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		3.4