5OCK
Crystal structure of ACPA E4 in complex with CEP1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-20 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.296, 101.048, 52.109 |
Unit cell angles | 90.00, 101.03, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.630 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.112 | 0.661 |
Rpim | 0.089 | 0.538 |
Number of reflections | 51683 | 2575 |
<I/σ(I)> | 6.7 | 1.8 |
Completeness [%] | 98.4 | 98.4 |
Redundancy | 3.7 | 3.7 |
CC(1/2) | 0.961 | 0.498 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% PEG3350, 0.2M ammonium citrate |