5OC8
HDM2 (17-111, WILD TYPE) COMPLEXED WITH NVP-HDM201 AT 1.56A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-01-26 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.99986 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 56.406, 56.406, 104.913 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.210 - 1.560 |
R-factor | 0.2382 |
Rwork | 0.237 |
R-free | 0.26030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ln2 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.220 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0063) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.210 | 19.210 |
High resolution limit [Å] | 1.560 | 1.560 |
Rmerge | 0.055 | 0.833 |
Rmeas | 0.057 | 0.858 |
Rpim | 0.054 | 0.422 |
Number of reflections | 14706 | |
<I/σ(I)> | 31.6 | 4 |
Completeness [%] | 99.9 | 100 |
Redundancy | 18.4 | 18.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298 | 3M AmSO4, 0.1M citrate |