5OAB
A novel crystal form of human RNase6 at atomic resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | I 2 3 |
Unit cell lengths | 95.405, 95.405, 95.405 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.703 - 1.111 |
R-factor | 0.1184 |
Rwork | 0.117 |
R-free | 0.14120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4x09 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.102 |
Data reduction software | XDS (20151001) |
Data scaling software | Aimless (0.5.17) |
Phasing software | PHENIX (1.11.1_2575) |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.703 | 1.151 |
High resolution limit [Å] | 1.111 | 1.111 |
Rmerge | 0.082 | 0.656 |
Rmeas | 0.094 | 0.813 |
Rpim | 0.044 | 0.469 |
Number of reflections | 54593 | 4253 |
<I/σ(I)> | 9.1 | 1.47 |
Completeness [%] | 96.2 | 75.17 |
Redundancy | 4 | 2.4 |
CC(1/2) | 0.996 | 0.544 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 1.3 M SODIUM/POTASSIUM PHOSPHATE |