5O8Y
Conformational dynamism for DNA interaction in Salmonella typhimurium RcsB response regulator.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-14 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97626 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 108.830, 108.830, 306.538 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 102.560 - 2.300 |
R-factor | 0.22484 |
Rwork | 0.223 |
R-free | 0.25274 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1a04 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.186 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 102.600 | 2.264 |
High resolution limit [Å] | 2.256 | 2.256 |
Rmerge | 0.175 | |
Rmeas | 0.179 | 2.958 |
Rpim | 0.035 | 0.652 |
Number of reflections | 87626 | 845 |
<I/σ(I)> | 17.9 | |
Completeness [%] | 100.0 | 92.2 |
Redundancy | 20 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 1.4M lithium sulfate 8% PEG1000 Hepes pH 7.5 |