5O7P
HER3 in complex with Fab MF3178
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-01 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97625 |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 141.131, 141.131, 320.817 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.987 - 4.500 |
R-factor | 0.2497 |
Rwork | 0.247 |
R-free | 0.29600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1m6b 3skj 4hcr |
RMSD bond length | 0.010 |
RMSD bond angle | 0.729 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11_2567: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.990 | 5.000 |
High resolution limit [Å] | 4.500 | 4.500 |
Rmerge | 0.200 | 1.400 |
Rpim | 0.066 | 0.460 |
Number of reflections | 11931 | 3286 |
<I/σ(I)> | 9.6 | 2.2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 10.9 | 11.3 |
CC(1/2) | 0.998 | 0.830 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M bis tris propane pH 7.5, 0.15 sodium citrate, 20% w/v PEG 3350 |