5O75
Ube4B U-box domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 110 |
Detector technology | PIXEL |
Collection date | 2016-12-17 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97628 |
Spacegroup name | P 6 2 2 |
Unit cell lengths | 80.180, 80.180, 39.525 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.090 - 1.483 |
R-factor | 0.1966 |
Rwork | 0.195 |
R-free | 0.22400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3l1z |
RMSD bond length | 0.008 |
RMSD bond angle | 1.029 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.438 | 1.509 |
High resolution limit [Å] | 1.483 | 1.483 |
Rmerge | 0.043 | 1.194 |
Rpim | 0.015 | 0.435 |
Number of reflections | 11868 | 636 |
<I/σ(I)> | 27.9 | 2.2 |
Completeness [%] | 91.9 | 100 |
Redundancy | 17 | 15 |
CC(1/2) | 1.000 | 0.771 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.1 M citric acid, pH 5.5, 1.9 M ammonium sulphate |