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5O5H

Crystal structure of the human BRPF1 bromodomain in complex with BZ053

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]100
Detector technologyPIXEL
Collection date2016-03-06
DetectorDECTRIS EIGER X 16M
Wavelength(s)1.000000
Spacegroup nameP 32 2 1
Unit cell lengths61.027, 61.027, 63.787
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution40.697 - 1.850
R-factor0.1944
Rwork0.190
R-free0.23460
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4lc2
RMSD bond length0.008
RMSD bond angle1.098
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX ((1.11.1_2575: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.7001.890
High resolution limit [Å]1.8501.850
Rmerge0.0410.640
Rpim0.0140.212
Number of reflections12134740
<I/σ(I)>43.95.4
Completeness [%]100.0100
Redundancy18.619.2
CC(1/2)1.0000.955
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2770.1 M Bis-Tris Propane, pH6.5, 0.2 M Sodium Nitrate, 20% PEG3350

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