5O57
Solution Structure of the N-terminal Region of Dkk4
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVIII | 600 | |
| 2 | Bruker | AVII | 800 | |
| 3 | Bruker | AVANCE III HD | 950 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 3D TROSY-HNCACB |
| 10 | 1 | 5 | 3D 13C/1H HSQC-NOESY |
| 11 | 1 | 2 | 3D 15N/1H NOESY-HSQC |
| 2 | 1 | 1 | 3D TROSY-HN(CO)CACB |
| 3 | 1 | 1 | 3D TROSY-HNCO |
| 4 | 1 | 1 | 3D HBHA(CO)NH |
| 5 | 1 | 1 | 2D TROSY |
| 6 | 1 | 3 | 2D 1H-1H TOCSY |
| 7 | 1 | 3 | 2D 1H-1H NOESY |
| 8 | 1 | 4 | 3D HCCH-TOCSY |
| 9 | 1 | 5 | 3D 13C/1H HSQC-NOESY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.5 | 1 | 308 |
Conformers
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 70 |
