5O0R
Deglycosylated Nogo Receptor with native disulfide structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-26 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.728, 111.654, 114.835 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.105 - 2.500 |
R-factor | 0.2546 |
Rwork | 0.252 |
R-free | 0.30260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ozn |
RMSD bond length | 0.002 |
RMSD bond angle | 0.547 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.730 | 2.640 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 21264 | |
<I/σ(I)> | 3.8 | 1.4 |
Completeness [%] | 98.8 | 99.8 |
Redundancy | 3.4 | 3.7 |
CC(1/2) | 0.981 | 0.663 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 291 | 1.8 M NaH2PO4/K2HPO4 pH 5.0 |