5NM6
Chicken GRIFIN (crystallisation pH: 4.6)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-06-06 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.943, 60.274, 54.145 |
Unit cell angles | 90.00, 92.47, 90.00 |
Refinement procedure
Resolution | 40.259 - 1.458 |
R-factor | 0.1783 |
Rwork | 0.176 |
R-free | 0.21740 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5nld |
RMSD bond length | 0.006 |
RMSD bond angle | 0.846 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.260 | 1.510 |
High resolution limit [Å] | 1.458 | 1.458 |
Rmerge | 0.093 | 0.560 |
Number of reflections | 39758 | 3661 |
<I/σ(I)> | 15.18 | 1.02 |
Completeness [%] | 91.0 | 84.47 |
Redundancy | 1.8 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295 | 30%PEG4K, Na Acetate 0.1M pH 4.6, 0.2M Amm. Sulfate |