5NLE
Chicken GRIFIN (crystallisation pH: 8.0)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-06-13 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.00 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 45.632, 103.976, 130.784 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.210 - 1.845 |
R-factor | 0.1866 |
Rwork | 0.184 |
R-free | 0.22620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5nld |
RMSD bond length | 0.008 |
RMSD bond angle | 1.169 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.210 | 1.910 |
High resolution limit [Å] | 1.840 | 1.840 |
Rmerge | 0.021 | 0.470 |
Number of reflections | 54344 | 5238 |
<I/σ(I)> | 14.12 | 1.66 |
Completeness [%] | 99.8 | 97.92 |
Redundancy | 2 | |
CC(1/2) | 0.630 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 295 | 10% PEG 3K, 0.1M Imidazole pH 8.0, 0.2M Li2SO4 |