5MUJ
BT0996 RGII Chain B Complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-15 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.976 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.460, 80.000, 50.810 |
Unit cell angles | 90.00, 114.94, 90.00 |
Refinement procedure
Resolution | 44.850 - 1.370 |
R-factor | 0.20077 |
Rwork | 0.198 |
R-free | 0.25181 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.709 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 44.850 |
High resolution limit [Å] | 1.370 |
Number of reflections | 74740 |
<I/σ(I)> | 1.4 |
Completeness [%] | 99.0 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% (w/v) PEG 3350 and 0.2 M Lithium Acetate |