5ME3
Structure of the Scc2 C-terminus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2015-02-14 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 98.049, 106.440, 143.183 |
Unit cell angles | 90.00, 104.52, 90.00 |
Refinement procedure
Resolution | 48.810 - 2.850 |
R-factor | 0.2201 |
Rwork | 0.217 |
R-free | 0.26910 |
Structure solution method | MIR |
RMSD bond length | 0.004 |
RMSD bond angle | 0.862 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | autoSHARP |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.810 | 2.952 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.071 | 1.244 |
Number of reflections | 65853 | |
<I/σ(I)> | 10.36 | 0.75 |
Completeness [%] | 99.0 | 96 |
Redundancy | 3.3 | 2.9 |
CC(1/2) | 0.312 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 100 mM imidazole (pH 6.8), 200 mM lithium sulphate, and 4.5% polyethylene glycol 5000 MME |