5MCB
Glycogen phosphorylase in complex with chlorogenic acid.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I911-2 |
Synchrotron site | MAX II |
Beamline | I911-2 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2015-09-05 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.043 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 128.950, 128.950, 116.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.950 |
R-factor | 0.14021 |
Rwork | 0.138 |
R-free | 0.17744 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5jtu |
RMSD bond length | 0.011 |
RMSD bond angle | 1.439 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.8.0151) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.980 |
High resolution limit [Å] | 1.950 | 1.950 |
Number of reflections | 52193 | |
<I/σ(I)> | 7.7 | 1.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.73 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 6.8 | 289 | 10mM BES Buffer |