5MA5
GFP-binding DARPin fusion gc_K11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-12-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 |
Unit cell lengths | 58.710, 60.280, 90.240 |
Unit cell angles | 86.94, 79.13, 89.35 |
Refinement procedure
Resolution | 44.249 - 1.850 |
R-factor | 0.1556 |
Rwork | 0.154 |
R-free | 0.18360 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.859 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11_2567: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.249 | 1.900 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.044 | 0.654 |
Number of reflections | 92746 | |
<I/σ(I)> | 18.31 | 2.46 |
Completeness [%] | 89.5 | 89.2 |
Redundancy | 3.74 | 3.76 |
CC(1/2) | 0.999 | 0.808 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1M tri Sodium citrate pH 5.6, 20% v/v 2-Propanol, 20%w/v PEG 4000 |