5LHB
POLYADPRIBOSYL GLYCOSIDASE IN COMPLEX WITH PDD00017262
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-07-11 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.010, 89.730, 95.440 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.610 - 2.230 |
R-factor | 0.1647 |
Rwork | 0.162 |
R-free | 0.21150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4a0d |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.510 | 2.370 |
High resolution limit [Å] | 2.230 | 2.230 |
Rmerge | 0.109 | 0.614 |
Number of reflections | 28669 | |
<I/σ(I)> | 8.6 | 3 |
Completeness [%] | 99.8 | 99.7 |
Redundancy | 5.7 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 25% PEG 3350, 36.4MM PCTP PH 4, 63.6MM PCTP PH 10, 0.2M AMMONIUM SULPHATE |