5LG7

Solution NMR structure of Tryptophan to Arginine mutant of Arkadia RING domain

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	SB Avance III		1000
2	Bruker	AVANCE		600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D HCCH-TOCSY
11	1	1	3D HNHA
12	1	2	2D 1H-13C HSQC
13	1	1	2D 1H-15N HSQC
14	1	1	3D 1H-15N NOESY
15	1	2	3D 1H-13C NOESY aliphatic
16	1	2	3D 1H-13C NOESY aromatic
17	1	2	4D APSY-HACANH
18	1	2	5D APSY-CBCACONH
19	1	2	5D APSY-HACACONH
2	1	2	3D CBCA(CO)NH
3	1	2	3D HNCA
4	1	2	3D HNCACB
5	1	2	3D HNCO
6	1	2	3D HBHA(CO)NH
7	1	1	3D 1H-15N NOESY
8	1	2	3D 1H-13C NOESY aliphatic
9	1	2	3D 1H-13C NOESY aromatic

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	1	298

Conformers

Conformers Calculated Total Number	31
Conformers Submitted Total Number	31