5KW9
Structural Basis for Norovirus Neutralization by a HBGA Blocking Human IgA Antibody
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2015-03-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.977 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 162.000, 162.000, 146.810 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 81.000 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.120 | 0.800 |
Number of reflections | 50863 | |
<I/σ(I)> | 15.1 | 3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11.1 | 10.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2M Sodium Formate, 0.1M Bis Tris propane, pH 6.5 and 20% w/v PEG3350 |