5KQD
PANK3:Palmitoyl-CoA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-03-21 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 0.979 |
Spacegroup name | P 2 3 |
Unit cell lengths | 121.707, 121.707, 121.707 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.487 - 2.600 |
R-factor | 0.1966 |
Rwork | 0.188 |
R-free | 0.20860 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3mk6 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.150 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.487 | 2.660 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.091 | 0.968 |
Number of reflections | 18791 | |
<I/σ(I)> | 21.2 | 1.4 |
Completeness [%] | 99.9 | 99.7 |
Redundancy | 5.4 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291.15 | Ammonium sulfate, Tris, PEG 600, Glycerol |