5KQ1
Crystal structure of S. pombe Dcp1/Dcp2 in complex with H. sapiens PNRC2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-09-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.115869 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.622, 118.727, 93.174 |
Unit cell angles | 90.00, 102.77, 90.00 |
Refinement procedure
Resolution | 44.494 - 3.002 |
R-factor | 0.212 |
Rwork | 0.210 |
R-free | 0.24740 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qkm |
RMSD bond length | 0.003 |
RMSD bond angle | 0.616 |
Data reduction software | HKL-2000 (v708c) |
Data scaling software | HKL-2000 (v708c) |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.050 |
High resolution limit [Å] | 3.000 | 8.130 | 3.000 |
Rmerge | 0.106 | 0.061 | 0.745 |
Number of reflections | 19125 | ||
<I/σ(I)> | 10.3 | ||
Completeness [%] | 99.0 | 96.2 | 91.9 |
Redundancy | 3.7 | 3.7 | 3.4 |
CC(1/2) | 0.990 | 0.796 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 150 mM trilithium citrate, 13% PEG 3350, 0.1% mellitic acid |