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5KA0

Protein Tyrosine Phosphatase 1B Delta helix 7, open state

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU FR-E+ SUPERBRIGHT
Temperature [K]100
Detector technologyCCD
Collection date2014-03-21
DetectorRIGAKU SATURN 944+
Wavelength(s)1.54
Spacegroup nameP 32 2 1
Unit cell lengths88.362, 88.362, 72.507
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution28.923 - 1.991
R-factor0.167
Rwork0.165
R-free0.21100
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3a5j
RMSD bond length0.011
RMSD bond angle1.047
Data scaling softwareHKL-2000
Phasing softwarePHASER (2.5.6)
Refinement softwarePHENIX
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.020
High resolution limit [Å]1.9905.4001.990
Rmerge0.0590.0390.219
Total number of observations465617
Number of reflections22728
<I/σ(I)>11.6
Completeness [%]99.899.497.5
Redundancy20.520.411.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.82770.1 M HEPES, pH 7.8, 0.2 M MgCl2, 12% PEG8000

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