5K7T

MicroED structure of thermolysin at 2.5 A resolution

Experimental procedure

Spacegroup name	P 61 2 2
Unit cell lengths	92.065, 92.065, 128.498
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	30.135 - 2.500
R-factor	0.291
Rwork	0.290
R-free	0.30960
RMSD bond length	0.003
RMSD bond angle	0.509
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	30.140	30.140	1.630
High resolution limit [Å]	1.600	8.630	1.600
Rmerge	0.634	0.206	0.794
Rpim	0.219	0.071	0.616
Number of reflections	25029	326	173
<I/σ(I)>	4	8.2	1
Completeness [%]	58.5	95.7	8
Redundancy	9	9.6	1.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1