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5JXH

Structure the proprotein convertase furin in complex with meta-guanidinomethyl-Phac-RVR-Amba at 2.0 Angstrom resolution.

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsBESSY BEAMLINE 14.1
Synchrotron siteBESSY
Beamline14.1
Temperature [K]100
Detector technologyPIXEL
Collection date2015-02-11
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.918409
Spacegroup nameP 65 2 2
格子定数 [Å]131.790, 131.790, 155.578
格子定数 [度]90.00, 90.00, 120.00
精密化法
残基43.138 - 2.000
R因子0.158
Rwork0.157
R-free0.18530
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4ryd
結合長の平均二乗偏差(RMSD) [Å]0.007
結合角の平均二乗偏差(RMSD) [度]1.042
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwarePHENIX (1.9_1692)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)43.1382.120
分解能 [Å] (高)2.0002.000
独立反射数53872
<I/σ(I)>13.48
完全性 [%]99.2
冗長性4.9
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, SITTING DROP293.15crystallization solution: 100 mM MES, 200 mM K/NaH2PO4, pH 5.5-6.0, 3-4 M NaCl, 3% DMSO; reservoir solution: 3-4 M NaCl

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件を2024-09-18に公開中

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