5JKW
HUMAN PLACENTAL AROMATASE CYTOCHROME P450 (CYP19A1) COMPLEXED WITH TESTOSTERONE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 140.523, 140.523, 118.471 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.500 - 3.000 |
R-factor | 0.19814 |
Rwork | 0.197 |
R-free | 0.22234 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 3s79 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.407 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.8.0131) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.500 |
High resolution limit [Å] | 3.000 |
Number of reflections | 24964 |
<I/σ(I)> | 23.3 |
Completeness [%] | 95.7 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 277 | 20-30% PEG 4000, PHOSPHATE BUFFER, PH 7.4 |