5JKE
Crystal structure of human IZUMO1-JUNO complex (crystal form 3)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-03-12 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0000 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 64.182, 141.776, 144.861 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.300 - 2.860 |
R-factor | 0.20429 |
Rwork | 0.203 |
R-free | 0.23817 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5jk9 5jka |
RMSD bond length | 0.011 |
RMSD bond angle | 1.592 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.300 |
High resolution limit [Å] | 2.860 |
Number of reflections | 31399 |
<I/σ(I)> | 28.5 |
Completeness [%] | 100.0 |
Redundancy | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% PEG4000, 0.2 M Li2SO4, 0.1 M MES-NaOH pH 6.0 |