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5JFS

Crystal structure of TrkA in complex with PF-00593174

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 17-ID
Synchrotron siteAPS
Beamline17-ID
Temperature [K]100
Detector technologyCCD
Collection date2010-03-09
DetectorADSC QUANTUM 210
Wavelength(s)1
Spacegroup nameP 64
Unit cell lengths125.220, 125.220, 46.510
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution24.300 - 2.070
R-factor0.171
Rwork0.170
R-free0.19090
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.010
RMSD bond angle1.030
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwareBUSTER
Refinement softwareBUSTER (2.9.3)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]107.4302.180
High resolution limit [Å]2.0702.070
Number of reflections24621
<I/σ(I)>12.3
Completeness [%]98.6
Redundancy6.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION277protein was concentrated to 10mg/ml. Crystals of complexes were grown using the hanging drop vapour diffusion method from 0.1M HEPES pH7.5, 0.1M MgCl2 and 10% EtOH at 4C

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