5JEO
Phosphorylated Rotavirus NSP1 in complex with IRF-3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 120 |
Detector technology | CCD |
Collection date | 2015-07-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 72.982, 72.982, 127.551 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.893 - 1.719 |
R-factor | 0.1698 |
Rwork | 0.169 |
R-free | 0.18320 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.005 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.893 | 1.750 |
High resolution limit [Å] | 1.719 | 1.720 |
Rmerge | 0.068 | |
Number of reflections | 42593 | |
<I/σ(I)> | 44.5 | 1.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11.8 | 10.9 |
CC(1/2) | 0.823 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M HEPES sodium pH7.5, 0.8 M NaH2PO4, 0.8 M KH2PO4 |