5JEM
Complex of IRF-3 with CBP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 2015-10-25 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.542 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 85.230, 88.660, 92.810 |
Unit cell angles | 90.00, 113.09, 90.00 |
Refinement procedure
Resolution | 36.992 - 2.500 |
R-factor | 0.1943 |
Rwork | 0.192 |
R-free | 0.24200 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.624 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 36.992 |
High resolution limit [Å] | 2.500 |
Number of reflections | 42426 |
<I/σ(I)> | 6.2 |
Completeness [%] | 96.3 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M HEPES pH 7.5, 25% PEG 3350 |