5JBQ
EF-TU (ESCHERICHIA COLI) IN COMPLEX WITH THIOMURACIN ANALOG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-04-30 |
Detector | RIGAKU SATURN 92 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 80.350, 125.340, 45.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.690 - 2.006 |
R-factor | 0.2069 |
Rwork | 0.204 |
R-free | 0.25270 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.160 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | BUSTER |
Refinement software | BUSTER (2.11.6) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.690 | 2.012 |
High resolution limit [Å] | 2.006 | 2.006 |
Rmerge | 0.065 | 0.250 |
Number of reflections | 31079 | |
<I/σ(I)> | 15.7 | 4.2 |
Completeness [%] | 98.5 | 66.2 |
Redundancy | 4.7 | 2.6 |
CC(1/2) | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.2 | 293 | 0.2M MgSO4, 18% PEG3350, 100mM Tris Cryo 20% Ethylene Glycol |