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5J4B

Crystal structure of the Thermus thermophilus 70S ribosome in complex with cisplatin (co-crystallized) and bound to mRNA and A-, P- and E-site tRNAs at 2.6A resolution

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-C
Synchrotron siteAPS
Beamline24-ID-C
Temperature [K]100
Detector technologyPIXEL
Collection date2015-11-05
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)0.97900
Spacegroup nameP 21 21 21
Unit cell lengths210.240, 450.360, 625.280
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution147.677 - 2.600
R-factor0.2198
Rwork0.217
R-free0.26390
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4y4p
RMSD bond length0.004
RMSD bond angle0.917
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX (1.8.2)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]365.439365.4392.670
High resolution limit [Å]2.60011.6302.600
Rmerge0.1200.0261.256
Rmeas0.1390.0301.465
Total number of observations6961850
Number of reflections178104920217130853
<I/σ(I)>8.828.721
Completeness [%]99.395.699.1
Redundancy3.909
CC(1/2)0.9960.9980.277
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION7.62920.1-0.2 M Arginine-HCl, 0.1M Tris-HCl pH 7.6, 2.5% PEG-20K, 7-12% MPD, 0.5 mM BME

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