5IT1

Streptomyces peucetius CYP105P2 complex with biphenyl compound

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2015-02-25
Detector	ADSC QUANTUM 270
Wavelength(s)	0.97934
Spacegroup name	C 1 2 1
Unit cell lengths	123.023, 122.941, 193.287
Unit cell angles	90.00, 90.03, 90.00

Refinement procedure

Resolution	50.000 - 2.100
R-factor	0.20247
Rwork	0.200
R-free	0.24297
RMSD bond length	0.019
RMSD bond angle	1.966
Data scaling software	HKL-2000
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0049)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.100
Number of reflections	165620
<I/σ(I)>	39.3
Completeness [%]	99.5
Redundancy	6.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	293	0.1 M Bis-Tris Propane, 0.2 M DL-Malic acid