5IM4

Crystal structure of designed two-component self-assembling icosahedral cage I52-32

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (3.5 Å)

Cell axes258.820258.820641.730
Cell angles90.0090.00120.00
SpacegroupH 3
Resolution limits110.72 - 3.50
the highest resolution shell value3.539 - 3.499
R-factor0.2275
R-work0.22690
the highest resolution shell value0.402
R-free0.23340
the highest resolution shell value0.390
RMSD bond length0.008
RMSD bond angle1.071

Data Collection Statistics

Resolution limits213.90 - 3.50
the highest resolution shell value -
Number of reflections200420
Rmerge_l_obs0.132
the highest resolution shell value0.674
Completeness99.1
Redundancy3.6
I/sigma(I)-3

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, HANGING DROP8298

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*