5IKC

X-RAY STRUCTURE OF THE N-TERMINAL DOMAIN OF HUMAN DOUBLECORTIN in complex with FAB

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X10SA
Synchrotron site	SLS
Beamline	X10SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-01-13
Detector	PSI PILATUS 6M
Wavelength(s)	1.000000
Spacegroup name	P 1 21 1
Unit cell lengths	66.858, 110.399, 75.092
Unit cell angles	90.00, 106.54, 90.00

Refinement procedure

Resolution	41.825 - 2.060
R-factor	0.2011
Rwork	0.198
R-free	0.26530
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	41.825		2.110
High resolution limit [Å]	2.060	9.210	2.060
Rmerge	0.149	0.033	1.407
Number of reflections	63983
<I/σ(I)>	7.33	33.26	0.96
Completeness [%]	99.1	97.1	97.2
Redundancy	3.3
CC(1/2)	0.991

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	unknown