5IJK
Crystal structure of anti-gliadin 1002-1E03 Fab fragment in complex of peptide PLQPEQPFP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-20 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.972 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 144.639, 144.639, 106.678 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.290 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 39676 | |
<I/σ(I)> | 21.5 | |
Completeness [%] | 99.9 | |
Redundancy | 8.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 2.256M (NH4)2SO4, 0.1M Citrate, pH 5.0 |