5IH1
Macrolide 2'-phosphotransferase type II - complex with GDP and phosphorylated josamycin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-08-12 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.370, 80.870, 97.870 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.867 - 1.310 |
R-factor | 0.1615 |
Rwork | 0.161 |
R-free | 0.17810 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.357 |
Data scaling software | XSCALE |
Refinement software | PHENIX (dev_1627) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 41.113 | 1.340 | |
High resolution limit [Å] | 1.310 | 5.860 | 1.310 |
Rmerge | 0.046 | 0.041 | 0.661 |
Number of reflections | 77829 | ||
<I/σ(I)> | 21.66 | 48.26 | 3.1 |
Completeness [%] | 100.0 | 99.7 | 100 |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 295 | 0.1 M calcium acetate, 0.1M Tris, 25-40% PEG 4000 |