5I7L
Crystal Structure of SPLUNC1 Disulfide Mutant M2 (A48C, V253C)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-17 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1.03319 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 47.083, 203.588, 120.211 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.842 - 2.598 |
R-factor | 0.2262 |
Rwork | 0.220 |
R-free | 0.28370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4kgh |
RMSD bond length | 0.009 |
RMSD bond angle | 1.505 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.842 | 2.691 |
High resolution limit [Å] | 2.598 | 2.598 |
Rmerge | 0.062 | 0.580 |
Number of reflections | 18284 | |
<I/σ(I)> | 21.33 | 4.34 |
Completeness [%] | 99.6 | 96.67 |
Redundancy | 5.1 | |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 310 | 6M Ammonium Nitrate, 0.1M Tris-HCL, pH 8.5 |