5HYF
Glycosylated Knob-Knob Fc fragment (P6122)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 97.466, 97.466, 107.061 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.210 - 1.800 |
R-factor | 0.19934 |
Rwork | 0.197 |
R-free | 0.24782 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5hye |
RMSD bond length | 0.020 |
RMSD bond angle | 2.425 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.210 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 28446 | |
<I/σ(I)> | 22.5 | 1.4 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 19.3 | 20 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 293 | 2.5 M sodium chloride, 0.1 M acetate |