5GTJ
CRYSTAL STRUCTURE OF CATALYTICALLY ACTIVE FORM OF HUMAN DUSP26
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2013-01-24 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97935 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 122.617, 100.803, 70.870 |
Unit cell angles | 90.00, 114.67, 90.00 |
Refinement procedure
Resolution | 39.691 - 2.000 |
R-factor | 0.1987 |
Rwork | 0.196 |
R-free | 0.25270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.910 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 39.691 |
High resolution limit [Å] | 2.000 |
Number of reflections | 53434 |
<I/σ(I)> | 17.7 |
Completeness [%] | 97.2 |
Redundancy | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 291 | 0.1M Tris-HCl pH 8.5, 0.9M potassium thiocyanate |